...... created the cal file by going line-out to line-in rather than from line-out to mic-in. Could that be a potential problem?
If I recalibrate the soundcard/pre using the mic-in, should I engage the phantom power button?
No, the line-out to line-in will be fine. If the soundcard cal file drops off quickly at 18K or is jagged, then that's as high as you should measure. If it tails off smoothly and slowly, then you can go higher. (read
this thread through on mic preamp calibration methods).
I'd like to see the graph though.
Really though, when you start to get serious about measurements above 15KHz in speakers, you should get a professional calibration done on the microphone. The generic files we supply are fine for sub woofers and general mid range work, but you're trying to get up to 20KHz without a properly calibrated mic....
brucek